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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1164002Generated: November 1, 2026

p-Toluenesulfonic acid → HCID 13066707, compound

https://huagongshe.com/reaction/1164002

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acidHCID 6101—
Reactant2-[2-Hydroxy-3-(2-chlorophenoxy)phenyl]acetic acidHCID 13066680—
SolventBenzeneHCID 241—
ProductHCID 13066707HCID 1306670767.5%

Reaction Steps

A mixture of 2-[2-hydroxy-3-(2-chlorophenoxy)phenyl]acetic acid (1.9 g) and p-toluenesulfonic acid (0.5 g) in benzene 50 ml was treated in a similar manner to that of Example 1-(6), and the residue was recrystallized from a mixture of diethyl ether and n-hexane to give 7-(2-chlorophenoxy)-2,3-dihydrobenzofuran-2-one (1.2 g). mp 118°-120° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04367238
Source datasetuspto-grants-1983_01
ORD IDord-69f008dfbfde476aa615417c08d405f0
Source noteuspto-grants-1983_01