HRID1164002

反应详情

EQUATION

反应方程式

HRID 1164002 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 2-[2-hydroxy-3-(2-chlorophenoxy)phenyl]acetic acid (1.9 g) and p-toluenesulfonic acid (0.5 g) in benzene 50 ml was treated in a similar manner to that of Example 1-(6), and the residue was recrystallized from a mixture of diethyl ether and n-hexane to give 7-(2-chlorophenoxy)-2,3-dihydrobenzofuran-2-one (1.2 g). mp 118°-120° C.

WORKUP

后处理

  1. additionwas treated in a similar manner to that of Example 1-(6)
  2. customthe residue was recrystallized from a mixture of diethyl ether and n-hexane