HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malonic Acid → HCID 54194699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 13066662 | HCID 13066662 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54194699 | HCID 54194699 | 53.3% |
Reaction Steps
2-Methoxy-3-(o-tolyloxy)benzaldehyde (28 g), malonic acid (24 g), pyridine (200 ml) and piperidine (2 ml) were treated in a similar manner to that of Example 4-(4), and the resultant crude product was crystallized with a mixture of benzene and n-hexane to give 3-[2-methoxy-3-(o-tolyloxy)phenyl]acrylic acid (17.5 g). mp 143°-146° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367238 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-7e6ef820848c470796bd66b812a89f43 |
| Source note | uspto-grants-1983_01 |