HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → Ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]valerate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20513486 | HCID 20513486 | — |
| Product | Ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]valerate | HCID 20513409 | 104% |
Reaction Steps
Sodium hydride (50%, 920 mg), ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]acetate (6 g) and n-propyl bromide (3.2 g) were treated in a similar manner to that of Example 10-(5) to give oily ethyl 2-cyano-2-[2-methoxy-3-(2-chlorophenoxy)phenyl]valerate (7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367238 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-d5cc01cc2c9d44d19ce860756ddec2e9 |
| Source note | uspto-grants-1983_01 |