HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromoheptane → HCID 20513493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20513460 | HCID 20513460 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20513493 | HCID 20513493 | 104.5% |
Reaction Steps
A suspension of sodium hydride (65%, 600 mg) in dimethylformamide (30 ml), a solution of ethyl 2-cyano-2-[2-methoxy-3-(o-tolyloxy)phenyl]acetate (5 g) in dimethylformamide (10 ml) and n-heptyl bromide (4.1 g) were treated in a similar manner to that of Example 25-(1) to give oily ethyl 2-cyano-2-[2-methoxy-3-(o-tolyloxy)phenyl]-n-nonanate (6.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367238 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-23cd40f915484e2596494c5b7ac50537 |
| Source note | uspto-grants-1983_01 |