HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13881506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,6-Dimethylaniline | HCID 6896 | — |
| Reactant | 1,3-Dibromobutane | HCID 7889 | — |
| Reactant | HCID 20512466 | HCID 20512466 | — |
| Product | HCID 13881506 | HCID 13881506 | 45.6% |
Reaction Steps
1,3-Bis(2',6'-dimethylphenyl-amino)-butane, applied as starting substance, can be prepared e.g. by the method of Shapiro et al. (loc. cit.), utilizing 2,6-dimethylaniline and 1,3-dibromobutane as starting materials. The free base boils at 159°-160° C./0.1 mm Hg, and the hydrochloride melts at 178°-180° C. Yield: 45.6%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04369325 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-cf6897643a9d41da8702d0daf9b101cc |
| Source note | uspto-grants-1983_01 |