HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(p-methoxyphenyl) telluroxide → 5alpha-Cholestan-3beta-ol benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(p-methoxyphenyl) telluroxide | HCID 3044917 | — |
| Reactant | HCID 178443927 | HCID 178443927 | — |
| Product | 5alpha-Cholestan-3beta-ol benzoate | HCID 86738769 | 93% |
Reaction Steps
5α-Cholestan-3β-ol-selenobenzoate (278 mg, 0.50 mmol) was reacted with bis-(p-methoxyphenyl)-telluroxide for 0.3 h. 5α-Cholestan-3β-ol-benzoate (229 mg, 93%) was obtained after p.l.c. (petroleum ether-ethyl acetate 9:1). The product obtained was recrystallized from ethyl acetate (198 mg, 80%) m.p. 136°-137° (lit., 136°-137°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04370497 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-28cb78dfe0bd4ebaa4a8240b499be37c |
| Source note | uspto-grants-1983_01 |