HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 86743792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 22164315 | HCID 22164315 | — |
| Product | HCID 86743792 | HCID 86743792 | — |
Reaction Steps
In analogy to Example 2, the N-cyclopropyl-2,4-dichlorothiazolesulphonamide was prepared by reacting 2,4-dichlorothiazole-sulphonyl chloride from Example 1 with anhydrous cyclopropylamine. Following recrystallization from toluene, 24.4 g of product were obtained (89.2% of the theoretical yield), m.p.: 90°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04906650 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-1466d134cfd6486d9b9ba11c863c0d66 |
| Source note | uspto-grants-1990_03 |