HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 22164314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | HCID 22164315 | HCID 22164315 | — |
| Product | HCID 22164314 | HCID 22164314 | — |
Reaction Steps
In analogy to Example 2, the N-allyl-2,4-dichlorothiazole-sulphonamide was prepared by reacting 2,4-dichlorothiazolesulphonyl chloride from Example 1 with anhydrous allylamine. Following recrystallization from petroleum ether/acetone (6:1), 7.6 g of product were obtained (28% of the theoretical yield), m.p.: 80°-81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04906650 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-dc4b9eb21bed44bf8803e6c2cca2fe9c |
| Source note | uspto-grants-1990_03 |