Stannous chloride dihydrate → HCID 19863381, compound

HRID 1164949Notes

Reaction equation

HRID 1164949 reaction equation
[CH2:1]([N:3]([CH2:19][CH2:20][CH2:21][CH2:22][CH:23]([CH3:25])[CH3:24])[CH2:4][CH2:5][N:6]([C:10]1[CH:15]=[CH:14][C:13]([N+:16]([O-])=O)=[CH:12][CH:11]=1)[CH2:7][CH:8]=[CH2:9])[CH3:2].O.O.[Sn](Cl)Cl>C(O)C>[NH2:16][C:13]1[CH:12]=[CH:11][C:10]([N:6]([CH2:7][CH:8]=[CH2:9])[CH2:5][CH2:4][N:3]([CH2:1][CH3:2])[CH2:19][CH2:20][CH2:21][CH2:22][CH:23]([CH3:24])[CH3:25])=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 61436Stannous chloride dihydrateHCID 19863363HCID 19863363, compound

Product 1

HCID 19863381HCID 19863381, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to Preparation 4 react N-ethyl-N-(5-methylhexyl)-N'-(4-nitrophenyl)-N'-(2-propenyl)1,2-ethanediamine with tin(II) chloride dihydrate in ethanol to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 4

Sources & evidence

ORD record
ord-7cc15a791af14e5a8b7a64e0a96ace21
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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