HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 19863364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | N-Ethyl-p-nitroaniline | HCID 19318 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | p-Toluenesulfonate | HCID 85570 | — |
| Product | HCID 19863364 | HCID 19863364 | — |
Reaction Steps
In a manner similar to Preparation 23 react 4-(hydroxymethyl)cyclohexanone with p-toluenesulfonyl chloride in pyridine to obtain the tosylate. The tosylate is further reacted with N-ethyl-4-nitrobenzenamine and sodium hydride in toluene as in Preparation 12 to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04906634 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-a77059a32cbd41a2b2f49e7d96d1febf |
| Source note | uspto-grants-1990_03 |