Stannous chloride dihydrate → HCID 19863412, compound

HRID 1164961Notes

Reaction equation

HRID 1164961 reaction equation
[CH2:1]([N:5]1[CH2:10][CH2:9][CH:8]([O:11][C:12]2[CH:17]=[CH:16][C:15]([N+:18]([O-])=O)=[C:14]([CH3:21])[CH:13]=2)[CH2:7][CH2:6]1)[CH2:2][CH2:3][CH3:4].O.O.[Sn](Cl)Cl>C(O)C>[NH2:18][C:15]1[CH:16]=[CH:17][C:12]([O:11][CH:8]2[CH2:7][CH2:6][N:5]([CH2:1][CH2:2][CH2:3][CH3:4])[CH2:10][CH2:9]2)=[CH:13][C:14]=1[CH3:21]

Participants

4

Reactant 2

HCID 61436Stannous chloride dihydrateHCID 19863442HCID 19863442, compound

Product 1

HCID 19863412HCID 19863412, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to Preparation 44 react 1-butyl-4-(3-methyl-4-nitrophenoxy)piperidine with tin(II) chloride dihydrate in ethanol to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 44

Sources & evidence

ORD record
ord-6300cb1098554b3dabaf073a9bdc180f
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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