N-Methylbenzylamine → HCID 19863448, compound

HRID 1164965Notes

Reaction equation

HRID 1164965 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]1[C:13]([Cl:14])=[CH:12][C:11]([N+:15]([O-:17])=[O:16])=[CH:10][C:9]=1[Cl:18].[CH3:19][NH:20][CH2:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[ClH:14].[Cl:18][C:9]1[CH:10]=[C:11]([N+:15]([O-:17])=[O:16])[CH:12]=[C:13]([Cl:14])[C:8]=1[O:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][N:20]([CH3:19])[CH2:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 7669N-Methylbenzylamine2×HCID 19863423HCID 19863423, compound

Product 1

HCID 19863448HCID 19863448, compound

Procedure

React 1-(5-bromopentyloxy)-2,6-dichloro-4-nitrobenzene with methyl(phenylmethyl)amine or benzyl(methyl)amine in a manner similar to Preparation 41 to obtain the title compound.

Workup

  1. customsimilar to Preparation 41

Sources & evidence

ORD record
ord-61dba1293b9b426e8509fd3c7dedf95c
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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