Stannous chloride dihydrate → HCID 19863417, compound

HRID 1164967Notes

Reaction equation

HRID 1164967 reaction equation
[CH2:1]([N:5]1[CH2:9][CH2:8][CH2:7][CH:6]1[CH2:10][O:11][C:12]1[CH:17]=[CH:16][C:15]([N+:18]([O-])=O)=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4].O.O.[Sn](Cl)Cl>C(O)C>[CH2:1]([N:5]1[CH2:9][CH2:8][CH2:7][CH:6]1[CH2:10][O:11][C:12]1[CH:17]=[CH:16][C:15]([NH2:18])=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 61436Stannous chloride dihydrateHCID 19863416HCID 19863416, compound

Product 1

HCID 19863417HCID 19863417, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to Preparation 44 react 1-butyl-2-[(4-nitrophenoxy)methyl]pyrrolidine with tin(II) chloride dihydrate in ethanol to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 44

Sources & evidence

ORD record
ord-626fe2bfd6ac469cb92fd150288e5aac
Source dataset
uspto-grants-1990_03
Patent number
US04906634

Reaction notes

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