HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54387892, compound → HCID 19863457, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54387892 | HCID 54387892 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19863457 | HCID 19863457 | — |
Reaction Steps
To 5.0 g (13.6 mmol) of 1-[2-[2-(diethylamino)ethoxy]-5-nitrophenyl]-3-phenyl-2-propen-1-one in 250 mL of ethanol add 0.5 g of palladium on carbon (10%). Hydrogenate the mixture at 22 psi until the theoretical amount of hydrogen has been absorbed. Filter the reaction and remove the solvent in vacuo to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04906634 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-855f11f993ef4e9fac3435435e3368e6 |
| Source note | uspto-grants-1990_03 |