Ethylenediamine → N-(2-Aminoethyl)-2-methylpropanamide

HRID 1164988노트

반응식

HRID 1164988 반응식
[CH2:1]([NH2:4])[CH2:2][NH2:3].[CH3:5][CH:6]([CH3:12])[C:7](OCC)=[O:8].NCC(N)(C)C>C(OCC)(=O)C>[CH3:5][CH:6]([CH3:12])[C:7]([NH:3][CH2:2][CH2:1][NH2:4])=[O:8]

참가 물질

5

반응물 3

HCID 3301EthylenediamineHCID 7342Ethyl isobutyrateHCID 131282-Methylpropylenediamine

생성물 1

HCID 12681828N-(2-Aminoethyl)-2-methylpropanamide

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

The procedure of Example IX was repeated in all essential details to produce the above compound, except that equivalent amounts of ethylenediamine and ethyl 2,2-dimethylacetate were substituted for 1,2-diamino-2-methylpropane and ethyl acetate, respectively. The product, which was identified by NMR and IR spectroscopy, was recovered as an oil.

후처리

  1. customto produce the above compound
  2. customwas recovered as an oil

출처 및 근거

ORD 기록
ord-e9c916c14e8643c59240cb644255fa3a
출처 데이터셋
uspto-grants-1990_03
특허 번호
US04906661

반응 노트

불러오는 중…