HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylindole → 2-(5-methyl-1H-indol-3-yl)-2-oxoacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylindole | HCID 11978 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(5-methyl-1H-indol-3-yl)-2-oxoacetyl chloride | HCID 12187418 | — |
Reaction Steps
Oxalyl chloride (0.76 ml) was slowly added to a stirred solution of 1 g of 5-methylindole in 20 ml of anhydrous ether at 0° C. The precipitate which formed was filtered off and dried at 80° C. to give 5-methyl-3-indolylglyoxylyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04906755 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-4d0502282b854029b6e941e39e0a32d6 |
| Source note | uspto-grants-1990_03 |