HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 70373898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 70373866 | HCID 70373866 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 70373898 | HCID 70373898 | 88.4% |
Reaction Steps
In a manner similar to Step E of Example 1, the reaction of 1.0 g (0.0026 mole) of N-[2-(thianaphthalene-2-yl)-2oxoethyl]-4-trifluoromethoxybenzamide with 0.53 g (0.0013 mole) of Lawesson's reagent in 25 ml of toluene yielded 0.45 g of 2-(4-trifluoromethoxyphenyl)-5-(thianaphthalene-2-yl)thiazole as a solid, mp 65-69, compound 40 of Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04908357 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-aead140f719549fd8598911580f1c399 |
| Source note | uspto-grants-1990_03 |