HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzyl alcohol → HCID 14072267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzyl alcohol | HCID 13397 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4,5-Dichloro-2-[4-(trifluoromethyl)phenyl]pyridazin-3(2H)-one | HCID 2774036 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14072267 | HCID 14072267 | 72.4% |
Reaction Steps
In 50 ml of N,N-dimethylformamide were dissolved 2.0 g (6.5 m mol) of 4,5-dichloro-2-(4-trifluoromethylphenyl)-3(2H)-pyridazinone and 0.92 g (6.5 m mol) of p-chlorobenzyl alcohol, and thereto was added 0.51 g of powdery potassium hydroxide. Then, the procedures in Synthesis Example 2 were repeated to give 1.94 g of the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04910201 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-0c6b556538d1453b835f1cee6966849a |
| Source note | uspto-grants-1990_03 |