HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzyl alcohol → HCID 14072382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzyl alcohol | HCID 13397 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4,5-Dichloro-2-(5-chloropyridin-2-yl)pyridazin-3(2H)-one | HCID 19861812 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14072382 | HCID 14072382 | 25.5% |
Reaction Steps
In 30 ml of N,N-dimethylformamide were dissolved 1.5 g (5.1 m mol) of 2-(5-chloropyridine-2-yl)-4,5-dichloropyridazinone and 0.73 g (5.1 m mol) of p-chlorobenzyl alcohol, and thereto was added 0.34 g of powdery potassium hydroxide. Then, the procedures in Synthesis Example 2 were repeated to give 500 mg of the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04910201 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-31fa828a93b845c6902c96462d505b4d |
| Source note | uspto-grants-1990_03 |