Acrylamide → HCID 11310181, compound

HRID 1165447Notes

Reaction equation

HRID 1165447 reaction equation
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[NH2:6][CH2:7][CH2:8][CH3:9]>CO>[CH2:7]([N:6]([CH2:3][CH2:2][C:1]([NH2:5])=[O:4])[CH2:3][CH2:2][C:1]([NH2:5])=[O:4])[CH2:8][CH3:9]

Participants

4

Reactant 2

HCID 6579AcrylamideHCID 7852Propylamine

Product 1

HCID 11310181HCID 11310181, compoundYield 97,590.398%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Conditions

Temperature
80 °C

Procedure

A mixture of 118.6 g (1.67 mol) of acrylamide and 49.3 g (0.83 mmol) of 1-aminopropane in 250 ml of methanol was heated at 80° C. for 1 hour. The solvent was evaporated and the solid crystallized from ethanol. There was obtained 162.3 g (0.81 mol, 97%) of 3,3'-(propylimino)bispropanamide as a white solid; mp 101°-101.5° C.

Workup

  1. customThe solvent was evaporated
  2. customthe solid crystallized from ethanol

Sources & evidence

ORD record
ord-fd260982f7b8469281d08f9dcc25effb
Source dataset
uspto-grants-1990_03
Patent number
US04910202

Reaction notes

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