Sodium → HCID 19833046, compound

HRID 1165458Notes

Reaction equation

HRID 1165458 reaction equation
[Na].[C:2](O)(=O)C.C[N:7]1[CH:13]2[CH2:14][C:15](=[N:17]O)[CH2:16][CH:8]1[CH2:9][CH2:10][CH2:11][CH2:12]2>>[CH3:2][NH:17][CH:15]1[CH2:14][CH:13]2[NH:7][CH:8]([CH2:9][CH2:10][CH2:11][CH2:12]2)[CH2:16]1

Participants

3

Reactant 2

HCID 5360545SodiumHCID 19833048HCID 19833048, compound

Product 1

HCID 19833046HCID 19833046, compound

Procedure

15 g of sodium are reacted in analogous manner to that disclosed below in Example (j) with 9.69 g 10-methyl-10-azabicyclo-[4.3.1]decan-8-one oxime acetate [m.pt. 253°-253.5° C. prepared in analogous manner to that disclosed in Example A-1b] giving an oil bpt 105°/0.9, mm after working up in conventional manner.

Workup

  1. customprepared in analogous manner to

Sources & evidence

ORD record
ord-28a94fec5c3042ca8458a4483586c3d5
Source dataset
uspto-grants-1990_03
Patent number
US04910207

Reaction notes

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