4-Bromobiphenyl → HCID 13799861, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][C:18]=1[O:19][CH3:20])[CH:6]=[CH:7][C:8]([N:10]1[CH2:15][CH2:14][O:13][CH2:12][CH2:11]1)=[O:9].Br[C:22]1[CH:27]=[CH:26][C:25]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)=[CH:24][CH:23]=1>>[C:25]1([C:28]2[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=2)[CH:26]=[CH:27][C:22](/[C:6](/[C:5]2[CH:16]=[CH:17][C:18]([O:19][CH3:20])=[C:3]([O:2][CH3:1])[CH:4]=2)=[CH:7]/[C:8]([N:10]2[CH2:11][CH2:12][O:13][CH2:14][CH2:15]2)=[O:9])=[CH:23][CH:24]=1Participants
3
Procedure
Analogous to Example 21, the title compound was prepared starting from 3,4-dimethoxycinnamic acid morpholide and 4-bromo-biphenyl.
Sources & evidence
- ORD record
- ord-73bbeadb21c9482586a18888e3626541
- Source dataset
- uspto-grants-1990_03
- Patent number
- US04910200
Reaction notes
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