HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylideneacetone → HCID 19862112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylideneacetone | HCID 637759 | — |
| Reactant | N-t-butyl-bis-(2-hydroxypropyl)amine | HCID 13930825 | — |
| Product | HCID 19862112 | HCID 19862112 | 56% |
Reaction Steps
N-t-butyl-bis-(2-hydroxypropyl)amine (60g, 0.32 mol) and trans-4-phenyl-3-buten-2-one (85g 10.58 mole) were subjected to a reaction as described in Example 1 above, except that the reaction temperature wa 220° C. A 56% yield of 3,4-dihydro-4-t-butyl-2,6-dimethyl-2H-1,4-oxazine was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04910303 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-76d2dbd6f4ef4824a33b5a62e9ef757a |
| Source note | uspto-grants-1990_03 |