HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dimethoxyethane → HCID 19862184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Reactant | HCID 19862185 | HCID 19862185 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 19862184 | HCID 19862184 | — |
Reaction Steps
51 g of 93% pure 1-benzyl-3-benzylamino-3-methylpyrrolidine-2,5-dione (0.154 mol) are reduced in 330 ml of dimethoxyethane using 12.4 g (0.33 mol) of lithium aluminum hydride. The work up is carried out as in A of Example 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04910319 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-17d9711e84b54987b615a614d05fa28e |
| Source note | uspto-grants-1990_03 |