Methylamine → HCID 14676891, compound

HRID 1165583Notes

Reaction equation

HRID 1165583 reaction equation
[CH:1]([C:3]1([CH3:17])[C:8]2[N:9]([CH3:16])[C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][C:15]=3[C:7]=2[S:6][CH2:5][CH2:4]1)=O.[CH3:18][NH2:19]>>[CH3:18][NH:19][CH2:1][C:3]1([CH3:17])[C:8]2[N:9]([CH3:16])[C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][C:15]=3[C:7]=2[S:6][CH2:5][CH2:4]1

Participants

3

Reactant 2

HCID 6329MethylamineHCID 14676889HCID 14676889, compound

Product 1

HCID 14676891HCID 14676891, compoundYield 97.4%

Procedure

In the same procedure as described in Example 2, 4-formyl-4,5-dimethyl-2,3,4,5-tetrahydrothiopyrano[3,2-b]indole is allowed to react with methylamine to give the title compound: Yield 97.4%.

Sources & evidence

ORD record
ord-9c2358e8b6b2408b8146ba55014ac6c9
Source dataset
uspto-grants-1990_03
Patent number
US04910318

Reaction notes

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