HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → HCID 14770227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | HCID 14770208 | HCID 14770208 | — |
| Solvent | Diethyl ether ethanol | HCID 21585056 | — |
| Product | HCID 14770227 | HCID 14770227 | 68.8% |
Reaction Steps
Using the procedure outlined in Example 1, benzo[b]naphtho[2,3-d]furan-11-carbaldehyde (2B) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave a 68.8% yield of 2-[[(benzo[b]naphtho[2,3-d]furan-11-yl)methyl]amino]-2-methyl-1,3-propanediol methanesuylfonate, mp 219°-220° (dec), (C,H,N,S), (EtOH/Et2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04910218 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-f13d8024635e49329640aa7217dcc88a |
| Source note | uspto-grants-1990_03 |