HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13752413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 13752411 | HCID 13752411 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13752413 | HCID 13752413 | — |
Reaction Steps
To a stirred solution containing 3 g methyl o-(4-isopropyl-4-methyl-5-thioxo-2-imidazolin-2-yl)-benzoate in 120 mL ether is added 0.867 mL concentrated HCl. After two hours, the precipitate was removed by filtration and dried under vacuum at 50° C. overnight. This material is analytically pure and has mp 195°-198° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04911747 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-38a7d2b64fc84859873663523cd1c923 |
| Source note | uspto-grants-1990_03 |