Hydrochloric Acid → HCID 13752413, compound

HRID 1165717Notes

Reaction equation

HRID 1165717 reaction equation
[CH:1]([C:4]1([CH3:20])[C:8](=[S:9])[NH:7][C:6]([C:10]2[CH:19]=[CH:18][CH:17]=[CH:16][C:11]=2[C:12]([O:14][CH3:15])=[O:13])=[N:5]1)([CH3:3])[CH3:2].[ClH:21]>CCOCC>[ClH:21].[CH:1]([C:4]1([CH3:20])[C:8](=[S:9])[NH:7][C:6]([C:10]2[CH:19]=[CH:18][CH:17]=[CH:16][C:11]=2[C:12]([O:14][CH3:15])=[O:13])=[N:5]1)([CH3:3])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 13752411HCID 13752411, compound

Product 1

HCID 13752413HCID 13752413, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To a stirred solution containing 3 g methyl o-(4-isopropyl-4-methyl-5-thioxo-2-imidazolin-2-yl)-benzoate in 120 mL ether is added 0.867 mL concentrated HCl. After two hours, the precipitate was removed by filtration and dried under vacuum at 50° C. overnight. This material is analytically pure and has mp 195°-198° C. (dec).

Workup

  1. customthe precipitate was removed by filtration
  2. customdried under vacuum at 50° C. overnight

Sources & evidence

ORD record
ord-38a7d2b64fc84859873663523cd1c923
Source dataset
uspto-grants-1990_03
Patent number
US04911747

Reaction notes

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