HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthaloyl chloride → tert-butyl N-(prop-2-en-1-yl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthaloyl chloride | HCID 6955 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | benzyl N-(prop-2-en-1-yl)carbamate | HCID 562279 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | tert-butyl N-(prop-2-en-1-yl)carbamate | HCID 4067274 | — |
Reaction Steps
N-benzyloxycarbonyl allyl amine was made in the same manner by utilizing benzyl chloroformate and triethylamine at 0° C. Cbz chloride, tosyl chloride, phthaloyl chloride and benzoyl chloride can similarly be used to obtain the corresponding allyl amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04912120 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-a0df6d9d8e344180977b0e39c0b1419b |
| Source note | uspto-grants-1990_03 |