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HRID1165914

反应详情

EQUATION

反应方程式

HRID 1165914 的结构方程式

REACTANTS

反应物

5
结构：O=C(Cl)c1ccccc1C(=O)Cl
HCID6955

1,2-Benzenedicarbonyl dichloride

C8H4Cl2O2

结构：Cc1ccc(S(=O)(=O)Cl)cc1
HCID7397

p-Toluenesulfonyl chloride

C7H7ClO2S

结构：O=C(Cl)c1ccccc1
HCID7412

Benzoyl chloride

C7H5ClO

结构：O=C(Cl)OCc1ccccc1
HCID10387

Benzyl chloroformate

C8H7ClO2

2 次

结构：C=CCNC(=O)OCc1ccccc1
HCID562279

Benzyl allylcarbamate

C11H13NO2

PRODUCTS

生成物

1
结构：C=CCNC(=O)OC(C)(C)C
HCID4067274

tert-Butyl hydrogen prop-2-en-1-ylcarbonimidate

C8H15NO2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

N-benzyloxycarbonyl allyl amine was made in the same manner by utilizing benzyl chloroformate and triethylamine at 0° C. Cbz chloride, tosyl chloride, phthaloyl chloride and benzoyl chloride can similarly be used to obtain the corresponding allyl amine.

WORKUP

后处理

  1. customat 0° C