Dimethylformamide → HCID 23050080, compound

HRID 1165916Notes

Reaction equation

HRID 1165916 reaction equation
[C:1]([O:5][C:6]([N:8]1[CH:12](CC)[CH:11](S)[CH:10]([CH2:16][NH2:17])[O:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].CN([CH:21]=[O:22])C>CO>[C:1]([O:5][C:6]([N:8]1[CH:12]([O:22][CH3:21])[CH2:11][CH:10]([CH2:16][NH2:17])[O:9]1)=[O:7])([CH3:2])([CH3:3])[CH3:4]

Participants

4

Reactant 2

HCID 6228DimethylformamideHCID 86743826HCID 86743826, compound

Product 1

HCID 23050080HCID 23050080, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In the same manner, N-tert-butoxycarbonyl-5-aminomethyl-3-ethylthiyl-4,5-dihydroisoxazole was made by using sodium ethyl thiolate in dry DMF instead of sodium methoxide in methanol.

Sources & evidence

ORD record
ord-f254d386c2f143f9b01c29d170dcd362
Source dataset
uspto-grants-1990_03
Patent number
US04912120

Reaction notes

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