HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylethylenimine → HCID 19861526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylethylenimine | HCID 9994 | — |
| Reactant | HCID 19861524 | HCID 19861524 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19861526 | HCID 19861526 | — |
Reaction Steps
7.66 g (50 mMol) N-ethyl-4-fluoro-3-methyl-aniline and 4.68 g (55 mMol) N-acetylaziridine are refluxed in 100 ml methanol (abs.) for 15 hours. Then the reaction mixture is evaporated on a rotary evaporator and the residue is digested with diisopropylether. The solid thus obtained is filtered with suction, washed with diisopropylether and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04912258 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-77d165d9394849129772a6dccf61dd0e |
| Source note | uspto-grants-1990_03 |