Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 2-(4-Chlorobenzoylamino)-3,4,5-trimethoxybenzoate | HCID 15406018 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178486767 | HCID 178486767 | — |
Reaction Steps
A suspension of 28.5 g of methyl 2-(4-chlorobenzoylamino)-3,4,5-trimethoxybenzoate in 200 ml of methanol was treated with 150 ml of liquid ammonia and heated at 100° C. for 5 h in an autoclave. On cooling, a precipitate deposited, which was filtered off with suction and dried under reduced pressure. Yield: 25 g. M.p.: 289° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06613772B1 |
|---|
| Source dataset | uspto-grants-2003_09 |
|---|
| ORD ID | ord-59b237c834a84dd6a45d0f96286e6094 |
|---|
| Source note | uspto-grants-2003_09 |
|---|
