HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 68920400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 68920401 | HCID 68920401 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68920400 | HCID 68920400 | — |
Reaction Steps
To a solution of 2-acetyloxybenzoic acid 6-(nitroxymethyl)-2-methylpyridinyl ester (1 g, 2.88 mmoles) in ethyl acetate (20 ml) cooled at 0° C., a solution of ethyl acetate/HCl 5M is added by dropping under stirring. It is left for one hour at 0° C., then the temperature is let reach room values. The formed precipitate is filtered and washed with ethyl ether. 900 mg of solid product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613784B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-336e4822f95748449d61ed0e893c453c |
| Source note | uspto-grants-2003_09 |