HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 22218336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | HCID 69659124 | HCID 69659124 | — |
| Product | HCID 22218336 | HCID 22218336 | 100% |
Reaction Steps
Following General Procedure D ethyl 4-(3-n-hexyloxy-5,5,8-trimethyl-5,6-dihydronaphthalen-2-ylamino)benzoate (Compound 112, 0.03 g, 0.07 mmol) was reacted with acetaldehyde and the resulting crude product, residue was purified by flash column chromatography (hexane:ethyl acetate=4:1) to afford 0.030 g (100%) of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613917B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-85457c16a12f44a4a3f751a60f9ddd10 |
| Source note | uspto-grants-2003_09 |