Potassium Carbonate → HCID 22999157, compound

HRID 1166724Notes

Reaction equation

HRID 1166724 reaction equation
[CH2:1]([C:4]1[CH:5]=[C:6]([CH:9]=[C:10]([O:13][CH3:14])[C:11]=1[OH:12])[CH:7]=[O:8])[CH:2]=[CH2:3].[CH:15]([C:18]1[CH:25]=[CH:24][C:21]([CH2:22]Cl)=[CH:20][CH:19]=1)([CH3:17])[CH3:16].C(=O)([O-])[O-].[K+].[K+]>CC(C)=O>[CH2:1]([C:4]1[CH:5]=[C:6]([CH:9]=[C:10]([O:13][CH3:14])[C:11]=1[O:12][CH2:22][C:21]1[CH:24]=[CH:25][C:18]([CH:15]([CH3:17])[CH3:16])=[CH:19][CH:20]=1)[CH:7]=[O:8])[CH:2]=[CH2:3]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 749164-Isopropylbenzyl chlorideHCID 15338063-Allyl-4-hydroxy-5-methoxy-benzaldehyde

Product 1

HCID 22999157HCID 22999157, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

The crude 3-allyl-4-hydroxy-5-methoxy-benzaldehyde was taken up in acetone and treated with 4-isopropylbenzyl chloride in the presence of potassium carbonate to give the desired product.

Sources & evidence

ORD record
ord-e0422c72db4046f7810b19b3c59d252c
Source dataset
uspto-grants-2003_09
Patent number
US06613942B1

Reaction notes

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