Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3-Methoxyphenyl)boronic acid → N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| 반응물 | N-(5-bromothiophenesulfonyl)pyrrole | HCID 23445587 | — |
| 생성물 | N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole | HCID 22998523 | 93% |
반응 단계
N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 3-methoxyphenylboronic acid and N-(5-bromothiophene-2-sulfonyl)pyrrole in 93% yield. This was purified by recrystallization using hexane/ethyl acetate as solvent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06613804B2 |
| 출처 데이터셋 | uspto-grants-2003_09 |
| ORD ID | ord-3fb080b7bc3847bfba90bacde221a72b |
| 출처 메모 | uspto-grants-2003_09 |