HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10497709, compound → HCID 10715441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10497709 | HCID 10497709 | — |
| Reactant | HCID 178425359 | HCID 178425359 | — |
| Product | HCID 10715441 | HCID 10715441 | 65% |
Reaction Steps
N-(3,4-dimethyl-5-isoxazolyl)-2-(4-tolylacetyl)thiophene-3-sulfonamide was prepared, as described in Example 93B, by reacting N-(3,4-dimethyl-5-isoxazolyl)-2-[N-methoxy(methylaminocarbonyl)]thiophene-3-sulfonamide with 4-methylbenzylmagnesium chloride, resulting in a 65% yield, m.p. 95-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613804B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-8b5e9be6cb7049f7ae48faba994504ca |
| Source note | uspto-grants-2003_09 |