Benzyl chloroformate → HCID 57190424, compound

HRID 1167222Notes

Reaction equation

FC(F)(F)C(O)=O.[S:8]1[CH:12]=[CH:11][C:10]([C:13]2[CH:18]=[CH:17][C:16]([CH:19]([CH3:22])[CH2:20][NH2:21])=[CH:15][CH:14]=2)=[CH:9]1.Cl[C:24]([O:26][CH2:27][C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1)=[O:25]>>[S:8]1[CH:12]=[CH:11][C:10]([C:13]2[CH:18]=[CH:17][C:16]([CH:19]([CH2:22][C:24]([O:26][CH2:27][C:28]3[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=3)=[O:25])[CH2:20][NH2:21])=[CH:15][CH:14]=2)=[CH:9]1

Participants

Reactant 2

HCID 10387Benzyl chloroformate

HCID 69594892HCID 69594892, compound

Product 1

HCID 57190424HCID 57190424, compound

Procedure

The title compound was prepared from 2-(4-(3-thienyl)phenyl)propyl amine trifluoroacetate (prepared in example 1) and benzyl chloroformate in a manner analogous to the procedure described in Example 1.

Sources & evidence

ORD record: ord-231d83f60b594668b3c5af8183a0ac6d
Source dataset: uspto-grants-2003_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06617351B1

Reaction notes

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