Dimethylcarbamoyl Chloride → HCID 9947887, compound

HRID 1167235Notes

Reaction equation

[S:1]1[CH:5]=[CH:4][C:3]([C:6]2[CH:11]=[CH:10][C:9]([CH:12]([CH3:15])[CH2:13][NH2:14])=[CH:8][CH:7]=2)=[CH:2]1.[CH3:16][N:17]([CH3:21])[C:18](Cl)=[O:19]>>[CH3:16][N:17]([CH3:21])[C:18]([NH:14][CH2:13][CH:12]([C:9]1[CH:10]=[CH:11][C:6]([C:3]2[CH:4]=[CH:5][S:1][CH:2]=2)=[CH:7][CH:8]=1)[CH3:15])=[O:19]

Participants

Reactant 2

HCID 6598Dimethylcarbamoyl Chloride

HCID 10727517HCID 10727517, compound

Product 1

HCID 9947887HCID 9947887, compound

Procedure

The title compound was prepared 2-(4-(3-thienyl)phenyl)propylamine (see example 14) and N,N-dimethylcarbamoyl chloride in a manner analogous to the procedure described in example 14. The NMR spectrum was consistent with the proposed title structure.

Sources & evidence

ORD record: ord-516c8548d7664d2eb8636979413d0328
Source dataset: uspto-grants-2003_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06617351B1

Reaction notes

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