Diethylcarbamoyl chloride → HCID 9883419, compound

HRID 1167236Notes

Reaction equation

[S:1]1[CH:5]=[CH:4][C:3]([C:6]2[CH:11]=[CH:10][C:9]([CH:12]([CH3:15])[CH2:13][NH2:14])=[CH:8][CH:7]=2)=[CH:2]1.[CH2:16]([N:18]([CH2:22][CH3:23])[C:19](Cl)=[O:20])[CH3:17]>>[CH2:16]([N:18]([CH2:22][CH3:23])[C:19]([NH:14][CH2:13][CH:12]([C:9]1[CH:10]=[CH:11][C:6]([C:3]2[CH:4]=[CH:5][S:1][CH:2]=2)=[CH:7][CH:8]=1)[CH3:15])=[O:20])[CH3:17]

Participants

Reactant 2

HCID 6916Diethylcarbamoyl chloride

HCID 10727517HCID 10727517, compound

Product 1

HCID 9883419HCID 9883419, compound

Procedure

The title compound was prepared from 2-(4-(3-thienyl)phenyl)propylamine (see example 14) and N,N-diethylcarbamoyl chloride in a manner analogous to the procedure described in example 14. The NMR spectrum was consistent with the proposed title structure.

Sources & evidence

ORD record: ord-b62e676feba047ffbcbacb7ccb244ff1
Source dataset: uspto-grants-2003_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06617351B1

Reaction notes

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