HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22996561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | N,N,2-trimethyl-5-nitro-Benzenesulfonamide | HCID 2921148 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22996561 | HCID 22996561 | 98% |
Reaction Steps
A suspension of 2-methyl-5-nitro(N,N-dimethyl)benzenesulfonamide (2.0 g, 8.20 mmol) and Pd/C (0.30 g) in ethanol (40 mL) was stirred under an H2 balloon for 16 h. The suspension was filtered through Celite and washed with methylene chloride. The filtrate was concentrated to provide 3-amino-2-methyl(N,N-dimethyl) benzenesulfonamide (1.72 g, 98%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06617357B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-d444b8205b9247d09527fa22a2447c68 |
| Source note | uspto-grants-2003_09 |