HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 69983093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | 2-Methylpentane | HCID 7892 | — |
| Reactant | HCID 69981542 | HCID 69981542 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 69983093 | HCID 69983093 | — |
Reaction Steps
Using essentially the technique of Example 113, starting from 3-(4-((3S)-3-amino-1-pyrrolidinyl)-3-fluorophenyl)-5(R)-(isoxazol-3-yloxymethyl)oxazolidin-2-one hydrochloride salt (170 mg, 0.43 mmol) and methyl chloroformate gave the desired product (114 mg) after trituration with diethyl ether and isohexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06617339B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-792640370df04b11963edfaf3fcd4939 |
| Source note | uspto-grants-2003_09 |