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HRID1167676

反应详情

EQUATION

反应方程式

HRID 1167676 的结构方程式

REACTANTS

反应物

2
结构：CO.Cl
HCID21893726

Hydrochloride methanol

CH5ClO

结构：CC(C)(C)OC(=O)NC[C@H](NC(=O)OCc1ccccc1)C(=O)OC(C)(C)C
HCID53876012

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC[C@H](N)C(=O)OC(C)(C)C.Cl
HCID86585733

未命名化合物

收率 99%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

13.1 g (33.2 mmol) of (13.8) are hydrogenated in methanol/HCl over 10% Pd/C. After 1.5 h, the mixture is filtered and the filtrate is concentrated in vacuo; 9.77 g (99%) of (13.9) are obtained as a colorless solid.

WORKUP

后处理

  1. filtrationthe mixture is filtered
  2. concentrationthe filtrate is concentrated in vacuo