HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 10228609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-(2-Hydroxyethyl)-2-pyrrolidinone | HCID 76980 | — |
| Reactant | 2-Chloro-N-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-isonicotinamide | HCID 11315694 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 10228609 | HCID 10228609 | — |
Reaction Steps
From 2-chloro-N-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-isonicotinamide with sodium hydride and 1-(2-hydroxyethyl)-2-pyrrolidone in dioxane. ES-MS m/e (%): 520 (M+Na+, 47), 498 (M+H+, 100). Analogously to Example 7 there were obtained:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620811B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-ad7df46219f7447b8a8ad273599f51e4 |
| Source note | uspto-grants-2003_09 |