HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methoxyphenyl)boronic acid → HCID 22994375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methoxyphenyl)boronic acid | HCID 201262 | — |
| Reactant | 4-Bromo-3-methylbenzonitrile | HCID 2737494 | — |
| Product | HCID 22994375 | HCID 22994375 | 80% |
Reaction Steps
4-Bromo-3-methylbenzonitrile and 4-methoxyphenylboronic acid were processed as described in Example 164A to provide the title compound (80% yield). 1HNMR (300 MHz, CDCl3) δ2.40 (3H), 3.73 (s, 3H), 6.84-7.60 (m, 7H); MS (DCI) m/z 224 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-8d3f6c2389db4461914abfb9190f3ac3 |
| Source note | uspto-grants-2003_09 |