HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenylboronic acid → HCID 22994464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenylboronic acid | HCID 2734326 | — |
| Reactant | 4-Bromo-2,6-difluorophenol | HCID 2736292 | — |
| Product | HCID 22994464 | HCID 22994464 | 48% |
Reaction Steps
4-Cyanophenylboronic acid and 4-bromo-2,6-difluorophenol were processed as described in Example 167A to provide the title compound (48% yield). 1HNMR (300 MHz, CDCl3) δ5.30 (bs, 1H), 7.20 (m, 2H), 7.60 (m, 2H), 7.78 (m, 2H); MS (CDI) m/z 232(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-7fb73a08c41443b88bdae66c12be49d1 |
| Source note | uspto-grants-2003_09 |