HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenylboronic acid → HCID 22994398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenylboronic acid | HCID 2734326 | — |
| Reactant | 4-Bromo-2-chloro-6-fluorophenol | HCID 2773270 | — |
| Product | HCID 22994398 | HCID 22994398 | 48% |
Reaction Steps
4-Cyanophenylboronic acid and 4-bromo-2-chloro-6-fluorophenol were processed as described in Example 167A to provide the title compound (48% yield). 1HNMR (300 MHz, MeOD) δ7.40 (m, 1H), 7.52 (m, 1H), 7.78 (s, 4H); MS (CDI) m/z 248 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-ccd2b798310f49eca3f586368dff70a3 |
| Source note | uspto-grants-2003_09 |