Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Triethyl Phosphate | HCID 6535 | — |
| Edukt | HCID 178448397 | HCID 178448397 | — |
| Produkt | HCID 178448396 | HCID 178448396 | 91,5% |
Reaktionsschritte
A solution containing di-tert-butylphenyliodonium chloride (443 mg; 1 mmol) and triethyl phosphate (3 g) was stirred at 110-120° C. for 1 hour. The thus-obtained solid matter was washed with ether, to thereby yield 432 mg of the target compound as white crystals (yield: 69.2%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06620957B1 |
|---|
| Quelldatensatz | uspto-grants-2003_09 |
|---|
| ORD ID | ord-aaef95135d264c25b33efc4e72280fec |
|---|
| Quellennotiz | uspto-grants-2003_09 |
|---|
